本源无机凝胶传输运移能力和封堵效果实验Tests of the transporting-migrating capacity and plugging effect for the origin inorganic gel
宋立志,郑华安,王闯,李彦闯,曹伟佳,卢祥国,吕鑫,梁守成,杨寨,张春生,高建崇
SONG Lizhi,ZHENG Huaan,WANG Chuang,LI Yanchuang,CAO Weijia,LU Xiangguo,Lü Xin,LIANG Shoucheng,YANG Zhai,ZHANG Chunsheng,GAO Jianchong
摘要(Abstract):
南海涠洲11-1油田经多年注水开发后储层非均质性进一步加剧,注入水低效无效循环现象日趋严重,亟待采取深部液流转向措施改善水驱开发效果。以油藏工程、高分子材料学和物理化学等为理论指导,以化学分析、仪器检测和物理模拟等为技术手段,以涠洲11-1油藏地质特征、流体性质和开发现状等为研究对象,开展了温度对无机凝胶基本性能影响,主剂质量浓度、段塞尺寸和注入轮次对无机凝胶传输运移和封堵效果影响实验研究,优化出了无机凝胶注入工艺参数。结果表明:无机凝胶具有较好的耐温性能,适用于南海涠洲11-1油田;随主剂段塞尺寸、注入轮次和质量浓度增大,注入端附近区域化学反应速度增加,无机凝胶分布量增加,传输运移能力变差;随隔离液段塞尺寸增加,主剂与注入水反应时间延后,岩心内无机凝胶分布更均匀,深部液流转向效果更好;在主剂用量相同条件下,与各轮次药剂采用"等浓"注入方式相比较,各轮次药剂采用"递增"注入方式时岩心内无机凝胶分布更均匀,深部液流转向效果更好。最优注入工艺参数为:主剂质量浓度为3 700~7 300 mg/L,主剂段塞尺寸为0.07~0.09 PV,隔离液段塞尺寸为0.014~0.021 PV,合理6轮次左右,主剂质量浓度合理递增幅度为610~980 mg/L。
After many years of the waterflooding development, the reservoir heterogeneity of Weizhou 11-1 Oilfield in the South China Sea has been further aggravated, and the low-effect and no-effect circulations of the injected water have become more and more serious. It is urgent to take deep fluid flow diverting measures to improve the waterflooding development effect. Based on the theoretical guidances of the reservoir engineering,ploymer material science and physical chemistry,taking the chemical analysis, instrument detection and physical simulation as the technical means and the geological characteristics, fluid properties and development status of Weizhou 11-1 reservoirs as the research objects,the test studies were carried out including the influence of the temperature on the properties of the inorganic gel and the effects of the agent concentration, slug size and injection cycle on the transporting-migrating and plugging effects,thus the injecting parameters of the inorganic gel were optimized. The results show that the inorganic gel with much better temperature resistance is suitable to Weizhou 11-1 Oilfield in the South China Sea.With the increase of the main slug size, injection cycle and mass concentration, the chemical reaction speed near the injected point increases as well, the distribution amount of the inorganic gel increases, and the transporting and migrating capacities become worse.With the increase of the slug size of the spacer,the reaction time of the main agent and the injected water is delayed, the distribution of the inorganic gel in the core is more uniform, and the deep fluid diversion effects are much better; under the condition of the same dosage of the main agent, compared with the "equal concentration" injecting method for each cycle of the agent, the distribution of the inorganic gel in the core is more uniform for "progressive increase" injecting mode of each cycle of the agent, and the deep fluid diversion effect can be much better. The optimal injecting parameters are shown as follows: the main agent concentration is 3 700~7 300 mg/L, the slug size of the main agent is 0.07~0.09 PV, the slug size of the spacer is 0.014~0.021 PV, the reasonable cycle is about 6 and the reasonable progressive increment of the main agent concentration is 610~980 mg/L.
关键词(KeyWords):
高温高盐油藏;无机凝胶;传输运移能力;封堵效果;参数优化;物理模拟;机理分析
high-temperature high-salt oil reservoir;inorganic gel;transporting-migrating capacity;plugging effect;parameter optimization;physical simulation;mechanism analysis
基金项目(Foundation): 中海石油(中国)有限公司湛江分公司重点攻关课题“涠洲11-1油田流三段无机凝胶涂层调剖调驱技术可行性研究(CCL2018ZJFN0800)、低渗注水开发油田调剖调驱技术分析测试”(CG2018ZCSYZX0034);中海石油(中国)有限公司综合科研项目“分级组合深部调剖技术扩大试验研究”(CCL2016RCPS0077RSN)
作者(Author):
宋立志,郑华安,王闯,李彦闯,曹伟佳,卢祥国,吕鑫,梁守成,杨寨,张春生,高建崇
SONG Lizhi,ZHENG Huaan,WANG Chuang,LI Yanchuang,CAO Weijia,LU Xiangguo,Lü Xin,LIANG Shoucheng,YANG Zhai,ZHANG Chunsheng,GAO Jianchong
DOI: 10.19597/j.issn.1000-3754.201909007
参考文献(References):
- [1]卢祥国,王树霞,王荣健,等.深部液流转向剂与油藏适应性研究:以大庆喇嘛甸油田为例[J].石油勘探与开发,2011,38(5):576-582.LU Xiangguo,WANG Shuxia,WANG Rongjian,et al.Adaptability of a deep profile control agent to reservoirs:Taking the Lamadian Oilfield in Daqing as an example[J].Petroleum Exploration and Development,2011,38(5):576-582.
- [2]何宏,王业飞,王国瑞,等.高温高盐油藏用调驱体系的研究进展[J].油田化学,2012,29(3):375-379.HE Hong,WANG Yefei,WANG Guorui,et al.Research advances in profile control and oil displacement agents for high temperature and high salinity reservoirs[J].Oilfield Chemistry,2012,29(3):375-379.
- [3]朱友益,侯庆锋,简国庆,等.化学复合驱技术研究与应用现状及发展趋势[J].石油勘探与开发,2013,40(1):90-96.ZHU Youyi,HOU Qingfeng,JIAN Guoqing,et al.Current development and application of chemical combination flooding technique[J].Petroleum Exploration and Development,2013,40(1):90-96.
- [4]苑光宇,侯吉瑞,罗焕,等.耐温抗盐调堵剂研究与应用进展[J].油田化学,2012,29(2):251-256.YUAN Guangyu,HOU Jirui,LUO Huan,et al.Research and application progress of high temperature resistant and high salinity tolerant plugging agents[J].Oilfield Chemistry,2012,29(2):251-256.
- [5]唐孝芬,吴奇,刘戈辉,等.区块整体弱凝胶调驱矿场试验及效果[J].石油学报,2003,24(4):58-61.TANG Xiaofen,WU Qi,LIU Gehui,et al.Field test on integral modifying and flooding project in regional reservoir with weak gel[J].Acta Petrolei Sinica,2003,24(4):58-61.
- [6]王小泉,魏君.一种硅酸类无机凝胶堵剂的制备[J].油田化学,2002,19(2):127-130.WANG Xiaoquan,WEI Jun.Preparation of cilicic inorganic gelatinous water control agent[J].Oilfield Chemistry,2002,19(2):127-130.
- [7]唐孝芬,刘玉章,常泽亮,等.适宜高温高盐地层的无机涂层调剖剂室内研究[J].石油勘探与开发,2004,31(6):92-94.TANG Xiaofen,LIU Yuzhang,CHANG Zeliang,et al.Profile modification agent with abio-gel coating for high-temperature and high-salinity reservoir[J].Petroleum Exploration and Development,2004,31(6):92-94.
- [8]赵彧,张桂意,崔洁,等.无机凝胶调剖剂的研制及应用[J].特种油气藏,2006,13(3):86-88.ZHAO Yu,ZHANG Guiyi,CUI Jie,et al.Development and application of inorganic gel profile control agent[J].Special Oil & Gas Reservoirs,2006,13(3):86-88.
- [9]张桂意,柴德民,崔洁,等.高温低渗油藏无机凝胶深部调剖剂WJ-2的研制[J].精细石油化工进展,2017,18(6):14-16.ZHANG Guiyi,CHAI Demin,CUI Jie,et al.Development of inorganic gel deep profile control agent WJ-2 for application in high-temperature low permeability reservoir[J].Advance in Fine Petrochemicais,2017,18(6):14-16.
- [10]牛丽伟,卢祥国,熊春明,等.无机凝胶成胶性能及封堵效果实验[J].石油勘探与开发,2013,40(6):728-732.NIU Liwei,LU Xiangguo,XIONG Chunming,et al.Experimental study on gelling property and plugging effect of inorganic gel system (OMGL) [J].Petroleum Exploration and Development,2013,40(6):728-732.
- [11]唐孝芬,杨立民,刘玉章,等.新型无机凝胶涂层深部液流转向剂[J].石油勘探与开发,2012,39(1):76-81.TANG Xiaofen,YANG Limin,LIU Yuzhang,et al.Inorganic gel coating in-depth fluid diverting agent[J].Petroleum Exploration and Development,2012,39(1):76-81.
- [12]唐孝芬,邵黎明,覃和,等.利用储层成垢离子物源实现优势通道调整提高水驱效率[J].油田化学,2018,35(2):257-262.TANG Xiaofen,SHAO Liming,QIN He,et al.Improvement of water flooding efficiency by using the reservoir forming ion source to realize the adjustment of the dominant channel[J].Oilfield Chemistry,2018,35(2):257-262.
- [13]卢祥国,高振环,闫文华,等.人造岩心渗透率影响因素试验研究[J].大庆石油地质与开发,1994,13(4):53-55.LU Xiangguo,GAO Zhenhuan,YAN Wenhua,et al.Experimental study of factors influencing permeability of articifical core[J].Petroleum Geology & Oilfield Development in Daqing,1994,13(4):53-55.
- [14]卢祥国,宋合龙,王景盛,等.石英砂环氧树脂胶结非均质模型制作方法:中国,ZL200510063665.8[P].2005-09-07.LU Xiangguo,SONG Helong,WANG Jingsheng,et al.Method for making heterogeneous model of quartz sand epoxy resin cementation:China,ZL200510063665.8[P].2005-09-07.
- 高温高盐油藏
- 无机凝胶
- 传输运移能力
- 封堵效果
- 参数优化
- 物理模拟
- 机理分析
high-temperature high-salt oil reservoir - inorganic gel
- transporting-migrating capacity
- plugging effect
- parameter optimization
- physical simulation
- mechanism analysis
- 宋立志
- 郑华安
- 王闯
- 李彦闯
- 曹伟佳
- 卢祥国
- 吕鑫
- 梁守成
- 杨寨
- 张春生
- 高建崇
SONG Lizhi - ZHENG Huaan
- WANG Chuang
- LI Yanchuang
- CAO Weijia
- LU Xiangguo
- Lü Xin
- LIANG Shoucheng
- YANG Zhai
- ZHANG Chunsheng
- GAO Jianchong
- 宋立志
- 郑华安
- 王闯
- 李彦闯
- 曹伟佳
- 卢祥国
- 吕鑫
- 梁守成
- 杨寨
- 张春生
- 高建崇
SONG Lizhi - ZHENG Huaan
- WANG Chuang
- LI Yanchuang
- CAO Weijia
- LU Xiangguo
- Lü Xin
- LIANG Shoucheng
- YANG Zhai
- ZHANG Chunsheng
- GAO Jianchong